8GOY
SulE P44R
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL18U1 |
| Synchrotron site | SSRF |
| Beamline | BL18U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-09-30 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.9791 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 51.353, 139.450, 58.125 |
| Unit cell angles | 90.00, 101.67, 90.00 |
Refinement procedure
| Resolution | 47.310 - 1.784 |
| Rwork | 0.159 |
| R-free | 0.18530 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4q34 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.918 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | PHENIX (v1.16) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.310 | 1.820 |
| High resolution limit [Å] | 1.780 | 1.780 |
| Number of reflections | 74840 | 3200 |
| <I/σ(I)> | 11.7 | |
| Completeness [%] | 98.3 | |
| Redundancy | 6.3 | |
| CC(1/2) | 0.997 | 0.572 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 277 | PEG 4000 |
