8GCH

GAMMA-CHYMOTRYPSIN IS A COMPLEX OF ALPHA-CHYMOTRYPSIN WITH ITS OWN AUTOLYSIS PRODUCTS

Experimental procedure

Spacegroup name	P 42 21 2
Unit cell lengths	69.000, 69.000, 95.300
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 * - 1.600
R-factor	0.193 *
RMSD bond angle	0.028 *

Data quality characteristics

	Overall
High resolution limit [Å]	1.600 *
Rmerge	0.024 *
Total number of observations	33900 *
Number of reflections	29204 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	5.5 *		Cohen, G.H., (1981) J. Mol. Biol., 148, 449. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	protein	12.5 (mg/ml)
2	1	1	ammonium sulfate	50 (%sat)