8FZO
Crystal structure of polyreactive 338E6 mouse Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-B |
Synchrotron site | APS |
Beamline | 23-ID-B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-02-06 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9791 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 40.920, 59.650, 82.250 |
Unit cell angles | 90.00, 99.10, 90.00 |
Refinement procedure
Resolution | 81.210 - 1.830 |
R-factor | 0.1748 |
Rwork | 0.172 |
R-free | 0.21970 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.885 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 81.210 | 1.895 |
High resolution limit [Å] | 1.830 | 1.830 |
Number of reflections | 33933 | 3289 |
<I/σ(I)> | 21.6 | |
Completeness [%] | 97.4 | |
Redundancy | 32.1 | |
CC(1/2) | 0.903 | 0.731 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 298 | 29% PEG 3000, 0.1M Sodium Sulfate, 0.1M Tris pH 8.5 |