8F9Q
Guinea pig sialic acid esterase (SIAE)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-15 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.0 |
Spacegroup name | P 64 |
Unit cell lengths | 206.554, 206.554, 155.190 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.610 - 2.760 |
R-factor | 0.188 |
Rwork | 0.188 |
R-free | 0.20430 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.797 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.860 |
High resolution limit [Å] | 2.760 | 2.760 |
Rmeas | 0.582 | |
Number of reflections | 192756 | 19184 |
<I/σ(I)> | 9 | |
Completeness [%] | 100.0 | |
Redundancy | 20.5 | |
CC(1/2) | 0.259 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 0.1 M MES, pH 6.5, 10% w/v PEG5000 MME, 12% v/v 1-propanol |