8EBF
C-terminal (TPR) domain of LIC11990 from Leptospira interrogans
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-02 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.97948 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.656, 100.093, 170.205 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.680 - 2.500 |
R-factor | 0.2377 |
Rwork | 0.235 |
R-free | 0.27760 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 0.860 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | CRANK2 |
Refinement software | BUSTER (2.10.4 (8-JUN-2022)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.680 | 2.540 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmeas | 0.090 | 1.800 |
Number of reflections | 29774 | 1503 |
<I/σ(I)> | 11.9 | 1 |
Completeness [%] | 96.5 | 98.8 |
Redundancy | 6.5 | 6 |
CC(1/2) | 0.999 | 0.600 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9 | 293 | 18% (w/v) PEG 3350, 0.3 M magnesium acetate |