8E0W

Crystal structure of mouse APCDD1 in P1 space group

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS-II BEAMLINE 17-ID-2
Synchrotron site	NSLS-II
Beamline	17-ID-2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-06-25
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.97933
Spacegroup name	P 1
Unit cell lengths	50.344, 65.599, 79.686
Unit cell angles	74.50, 76.82, 72.23

Refinement procedure

Resolution	33.930 - 2.150
R-factor	0.1814
Rwork	0.179
R-free	0.21980
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	8e0p
Data reduction software	xia2
Data scaling software	autoPROC
Phasing software	PHASER
Refinement software	PHENIX (1.19.2_4158)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	37.902	2.370
High resolution limit [Å]	2.144	2.144
Rmerge	0.087	0.367
Rpim	0.052	0.231
Number of reflections	34100	1705
<I/σ(I)>	11.2	1
Completeness [%]	91.2	59.3
Redundancy	3.7	3.5
CC(1/2)	0.992	0.886

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION	5.8	293	0.1 M magnesium acetate, 0.1 M sodium citrate, pH 5.8, 14% PEG5000 MME