8DAG
[8 bp center] Self-Assembled 3D DNA Hexagonal Tensegrity Triangle
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-12 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 1.00743 |
Spacegroup name | P 63 |
Unit cell lengths | 130.428, 130.428, 53.404 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.690 - 6.160 |
R-factor | 0.1213 |
Rwork | 0.120 |
R-free | 0.12670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7r96 |
RMSD bond length | 0.016 |
RMSD bond angle | 1.599 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 65.210 | 7.020 |
High resolution limit [Å] | 6.160 | 6.160 |
Number of reflections | 1054 | 211 |
<I/σ(I)> | 10.7 | |
Completeness [%] | 89.3 | |
Redundancy | 19.8 | |
CC(1/2) | 0.996 | 0.344 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9.5 | 293 | 1.75 M ammonium sulfate, 120 mM Tris, 120 mM Acetic Acid, 6 mM EDTA |