8CYM
[2T7+9bp Linker] Self-Assembled 3D DNA Hexagonal Tensegrity Triangle with 9 bp Sticky-End Linker
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-06-13 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 1.00743 |
Spacegroup name | P 63 |
Unit cell lengths | 173.130, 173.130, 87.833 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.980 - 7.760 |
R-factor | 0.0808 |
Rwork | 0.079 |
R-free | 0.11300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7r96 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.001 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 86.570 | 8.840 |
High resolution limit [Å] | 7.760 | 7.760 |
Number of reflections | 1347 | 191 |
<I/σ(I)> | 5.1 | |
Completeness [%] | 87.0 | |
Redundancy | 9.8 | |
CC(1/2) | 1.000 | 0.389 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 1.75 M ammonium sulfate, 120 mM Tris, 120 mM Acetic Acid, 6 mM EDTA |