8CS1
[GA/CT] Self-Assembled 3D DNA Hexagonal Tensegrity Triangle
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-02-21 |
Detector | DECTRIS EIGER2 S 9M |
Wavelength(s) | 1.00743 |
Spacegroup name | P 63 |
Unit cell lengths | 123.316, 123.316, 57.154 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.010 - 4.560 |
R-factor | 0.2144 |
Rwork | 0.214 |
R-free | 0.22060 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7r96 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.632 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.010 | 4.900 |
High resolution limit [Å] | 4.560 | 4.560 |
Number of reflections | 2373 | 200 |
<I/σ(I)> | 15.1 | |
Completeness [%] | 90.4 | |
Redundancy | 20.3 | |
CC(1/2) | 0.999 | 0.551 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9.5 | 293 | 1.83 M ammonium sulfate, 120 mM Tris, 120 mM Acetic Acid, 6 mM EDTA |