8CGQ
Crystal structure of UGT708A6 with UDP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | MAX IV BEAMLINE BioMAX |
| Synchrotron site | MAX IV |
| Beamline | BioMAX |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-09-25 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.9763 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 51.431, 72.593, 57.018 |
| Unit cell angles | 90.00, 101.69, 90.00 |
Refinement procedure
| Resolution | 44.260 - 2.040 |
| R-factor | 0.1802 |
| Rwork | 0.178 |
| R-free | 0.22710 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.099 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.260 | 2.120 |
| High resolution limit [Å] | 2.040 | 2.040 |
| Rmerge | 0.108 | 0.925 |
| Rmeas | 0.117 | 1.063 |
| Rpim | 0.046 | 0.510 |
| Number of reflections | 25283 | 2028 |
| <I/σ(I)> | 10.1 | 1.22 |
| Completeness [%] | 96.7 | 77.62 |
| Redundancy | 6.4 | 4.1 |
| CC(1/2) | 0.998 | 0.603 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 295 | PEG 3350 20% w/v, BIS-TRIS propane 100mM, |
