8C0D
UFL1/DDRGK1 bound to UFC1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-09 |
Detector | DECTRIS PILATUS3 X 2M |
Wavelength(s) | 0.873128 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 79.210, 124.565, 131.292 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 65.732 - 2.564 |
Rwork | 0.232 |
R-free | 0.28580 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.888 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0403) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 65.732 | 2.892 |
High resolution limit [Å] | 2.564 | 2.564 |
Number of reflections | 25858 | 1293 |
<I/σ(I)> | 8.2 | |
Completeness [%] | 93.8 | |
Redundancy | 12.8 | |
CC(1/2) | 0.997 | 0.674 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.2 | 292 | 0.1M HEPES, 1.03M Li2SO4 |