8AJI
Crystal structure of DltE from L. plantarum, TCEP form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-18 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.873130 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 76.236, 98.642, 135.934 |
Unit cell angles | 90.00, 105.80, 90.00 |
Refinement procedure
Resolution | 49.501 - 1.940 |
Rwork | 0.183 |
R-free | 0.21240 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 8agr |
RMSD bond length | 0.008 |
RMSD bond angle | 1.397 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0352) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.501 | 1.970 |
High resolution limit [Å] | 1.940 | 1.940 |
Rmerge | 0.095 | 0.395 |
Number of reflections | 139757 | 6771 |
<I/σ(I)> | 5.3 | |
Completeness [%] | 97.7 | |
Redundancy | 3.8 | |
CC(1/2) | 0.988 | 0.811 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | PEG 3350, ammonium tartrate, TCEP HCl |