7ZVU
HUMAN PRMT5:MEP50 Crystal Structure With MTA and Fragment Bound
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-07-03 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.9197 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 105.152, 139.162, 178.511 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 109.750 - 1.950 |
R-factor | 0.2384 |
Rwork | 0.237 |
R-free | 0.26580 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5eml |
RMSD bond length | 0.014 |
RMSD bond angle | 1.803 |
Data reduction software | XDS (Feb 5, 2021 (BUILT 20210323)) |
Data scaling software | Aimless (0.7.7) |
Phasing software | REFMAC (5.8.0267) |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 109.780 | 2.174 |
High resolution limit [Å] | 1.946 | 1.946 |
Number of reflections | 60214 | 3012 |
<I/σ(I)> | 13.8 | |
Completeness [%] | 95.0 | 75.5 |
Redundancy | 12.1 | |
CC(1/2) | 0.990 | 0.790 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 281 | 14% PEG3350, 100 mM Na citrate pH 5.4, 100mM Carboxylic acids |