7ZUT
Penicillium expansum chimera loop1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2021-10-28 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97918 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 44.931, 44.931, 42.829 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.910 - 1.100 |
R-factor | 0.127 |
Rwork | 0.126 |
R-free | 0.14590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7ztf |
RMSD bond length | 0.008 |
RMSD bond angle | 1.421 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.830 | 1.160 |
High resolution limit [Å] | 1.100 | 1.100 |
Rmerge | 0.049 | 0.110 |
Rpim | 0.012 | 0.035 |
Number of reflections | 20337 | 2596 |
<I/σ(I)> | 40.8 | |
Completeness [%] | 98.0 | |
Redundancy | 17.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 294 | 3.5M ammonium sulphate, 1% MPD, 0.1M Mes pH 6.5 |