7ZTY
Structure of Vps39 N-terminal domain from Chaetomium thermophilum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-05 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97937 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 64.700, 102.750, 59.560 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.230 - 2.890 |
R-factor | 0.2701 |
Rwork | 0.269 |
R-free | 0.29820 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | ALPHAFOLD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.551 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.820 | 3.070 |
High resolution limit [Å] | 2.890 | 2.890 |
Rmeas | 0.231 | 1.240 |
Number of reflections | 17010 | 2619 |
<I/σ(I)> | 7.7 | 1.8 |
Completeness [%] | 99.1 | |
Redundancy | 6.72 | |
CC(1/2) | 0.993 | 0.766 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 285 | 20% PEG MME 2000, 0.1 M MES pH 7.25 |