7ZSZ
Crystal structure of the GH11 domain of a multidomain xylanase from the hindgut metagenome of Trinervitermes trinervoides
Replaces: 7AYLExperimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-14 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.976 |
Spacegroup name | P 1 |
Unit cell lengths | 38.490, 43.420, 69.900 |
Unit cell angles | 100.87, 96.36, 116.00 |
Refinement procedure
Resolution | 37.310 - 1.500 |
R-factor | 0.1822 |
Rwork | 0.180 |
R-free | 0.21660 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7AYL |
RMSD bond length | 0.006 |
RMSD bond angle | 0.886 |
Data reduction software | XDS (1.12_2829) |
Data scaling software | xia2 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.310 | 1.413 |
High resolution limit [Å] | 1.390 | 1.390 |
Rmerge | 0.049 | 0.278 |
Number of reflections | 68762 | 2652 |
<I/σ(I)> | 13.6 | |
Completeness [%] | 87.5 | 67 |
Redundancy | 1.6 | 1.6 |
CC(1/2) | 0.999 | 0.816 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.8 | 293.15 | Na acetate, (NH4)2SO4 |