7ZOW
Crystal structure of Synechocystis halorhodopsin (SyHR), Cl-pumping mode, O state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-10-14 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.976 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 62.406, 62.406, 110.076 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.280 - 1.600 |
R-factor | 0.1969 |
Rwork | 0.195 |
R-free | 0.23160 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4hyj |
RMSD bond length | 0.006 |
RMSD bond angle | 0.869 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.520 | 48.520 | 1.640 |
High resolution limit [Å] | 1.600 | 7.160 | 1.600 |
Rmeas | 0.227 | 0.069 | 2.988 |
Number of reflections | 33454 | 443 | 2440 |
<I/σ(I)> | 6.6 | 21.7 | 0.8 |
Completeness [%] | 100.0 | 98 | 100 |
Redundancy | 11.1 | 9.5 | 11 |
CC(1/2) | 0.998 | 0.999 | 0.289 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 4.6 | 293 | 1.6 M Ammonium Phosphate |