7ZJR
X-ray structure of the periplasmic region of PilJ from P. aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-09-04 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 80.059, 80.059, 202.994 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.440 - 2.503 |
R-factor | 0.216598906847 |
Rwork | 0.215 |
R-free | 0.24524 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2yfa |
RMSD bond length | 0.009 |
RMSD bond angle | 0.904 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.440 | 2.460 |
High resolution limit [Å] | 2.320 | 2.320 |
Rmeas | 0.068 | 1.960 |
Number of reflections | 54408 | 8751 |
<I/σ(I)> | 21.36 | 1.07 |
Completeness [%] | 99.9 | |
Redundancy | 7.8 | |
CC(1/2) | 0.450 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 30% v/v Jeffamine M-600 pH 7.0, 0.1 M Tris pH 8.5 |