7ZGT
C-Methyltransferase PsmD from Streptomyces griseofuscus (apo form)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-06-30 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0332 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 71.050, 87.490, 89.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.880 - 2.050 |
R-factor | 0.2172 |
Rwork | 0.215 |
R-free | 0.25240 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1wzn |
RMSD bond length | 0.002 |
RMSD bond angle | 0.415 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.880 | 2.100 |
High resolution limit [Å] | 2.050 | 2.050 |
Rmeas | 0.117 | 4.329 |
Number of reflections | 35369 | 2572 |
<I/σ(I)> | 17.16 | 0.8 |
Completeness [%] | 99.6 | 99.3 |
Redundancy | 13.07 | 13.51 |
CC(1/2) | 1.000 | 0.354 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | magnesium formate |