7Z9A

Sam68

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-11-29
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97926
Spacegroup name	P 41 2 2
Unit cell lengths	96.984, 96.984, 83.721
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	43.410 - 2.570
Rwork	0.200
R-free	0.22790
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5emo
RMSD bond length	0.010
RMSD bond angle	2.110
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	MOLREP
Refinement software	REFMAC (5.8.0267)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	43.410	2.680
High resolution limit [Å]	2.570	2.570
Number of reflections	13222	1593
<I/σ(I)>	16
Completeness [%]	99.7
Redundancy	8.3
CC(1/2)	0.999	0.527

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	Ammonium sulfate