7Z6W
Complex of E. coli LolA and lipoprotein
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-08 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.91587 |
Spacegroup name | I 4 |
Unit cell lengths | 90.980, 90.980, 47.560 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 64.330 - 1.840 |
R-factor | 0.1829 |
Rwork | 0.181 |
R-free | 0.21620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ua8 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.721 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless (0.7.7) |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 64.330 | 64.330 | 1.880 |
High resolution limit [Å] | 1.840 | 9.010 | 1.840 |
Rmerge | 0.124 | 0.029 | 1.374 |
Rmeas | 0.130 | 0.030 | 1.433 |
Rpim | 0.037 | 0.008 | 0.405 |
Total number of observations | 207055 | 2079 | 12981 |
Number of reflections | 17042 | 164 | 1036 |
<I/σ(I)> | 14.3 | 57.9 | 2 |
Completeness [%] | 100.0 | 99.8 | 100 |
Redundancy | 12.1 | 12.7 | 12.5 |
CC(1/2) | 0.999 | 1.000 | 0.536 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 288.15 | 2.1 M DL-Malic acid pH 6.0 |