7Z6M
Crystal structure of Zn2+-transporter BbZIP in a cadmium bound state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-12-09 |
Detector | DECTRIS EIGER R 4M |
Wavelength(s) | 1 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 96.211, 61.656, 55.262 |
Unit cell angles | 90.00, 108.90, 90.00 |
Refinement procedure
Resolution | 45.510 - 2.510 |
R-factor | 0.2345 |
Rwork | 0.230 |
R-free | 0.27830 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5tsa |
RMSD bond length | 0.008 |
RMSD bond angle | 1.082 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.510 | 2.600 |
High resolution limit [Å] | 2.510 | 2.510 |
Rmerge | 0.163 | |
Rmeas | 0.175 | |
Rpim | 0.063 | 0.881 |
Number of reflections | 10448 | 1011 |
<I/σ(I)> | 8.56 | |
Completeness [%] | 98.6 | 96.65 |
Redundancy | 7.6 | 7.1 |
CC(1/2) | 0.998 | 0.410 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 7.4 | 291 | 100 mM HEPES-NaOH pH = 7.4, 100 mM CdCl2, 30% and PEG400 |