7Z3H
Crystal structure of Iba57 from Chaetomium thermophilum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-02-27 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97856 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 96.530, 134.180, 107.010 |
Unit cell angles | 90.00, 97.59, 90.00 |
Refinement procedure
Resolution | 47.340 - 2.400 |
R-factor | 0.2398 |
Rwork | 0.238 |
R-free | 0.27350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ESR |
RMSD bond length | 0.003 |
RMSD bond angle | 0.633 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.340 | 2.486 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.100 | 1.474 |
Number of reflections | 104927 | 10450 |
<I/σ(I)> | 9.19 | 1.08 |
Completeness [%] | 99.5 | |
Redundancy | 3.7 | |
CC(1/2) | 0.995 | 0.357 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 294 | 0.1 M Citric acid pH 4.0 5 % (w/v) PEG 6000 |