7YTF
Structure of OCPx2 from Nostoc flagelliforme CCNUN1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-13 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.979183 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 154.635, 154.635, 86.866 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.680 - 2.650 |
R-factor | 0.2017 |
Rwork | 0.199 |
R-free | 0.25650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4xb5 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.653 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0257) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 66.960 | 2.780 |
High resolution limit [Å] | 2.650 | 2.650 |
Rmerge | 0.099 | 0.781 |
Number of reflections | 18058 | 2372 |
<I/σ(I)> | 29.5 | 5.9 |
Completeness [%] | 98.6 | 100 |
Redundancy | 39.3 | |
CC(1/2) | 0.999 | 0.985 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1 M BIS-TRIS pH 5.5, 2.0 M Ammonium sulfate |