7YPF
Crystal structure of AsfvPCNA in space group of P1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2020-11-26 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.9793 |
Spacegroup name | P 1 |
Unit cell lengths | 54.659, 118.873, 118.843 |
Unit cell angles | 60.03, 89.98, 89.96 |
Refinement procedure
Resolution | 29.730 - 2.500 |
R-factor | 0.2094 |
Rwork | 0.208 |
R-free | 0.23250 |
Structure solution method | SAD |
RMSD bond length | 0.004 |
RMSD bond angle | 1.019 |
Data reduction software | iMOSFLM |
Data scaling software | HKL-2000 |
Phasing software | AutoSol |
Refinement software | PHENIX ((1.19.1_4122: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 30.000 | 2.590 |
High resolution limit [Å] | 2.500 | 5.380 | 2.500 |
Rmerge | 0.052 | 0.039 | 0.406 |
Rmeas | 0.061 | 0.045 | 0.496 |
Rpim | 0.032 | 0.024 | 0.280 |
Total number of observations | 286920 | ||
Number of reflections | 87599 | 8900 | 8393 |
<I/σ(I)> | 11.2 | ||
Completeness [%] | 97.5 | 99 | 93.3 |
Redundancy | 3.3 | 3.5 | 2.8 |
CC(1/2) | 0.995 | 0.680 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1 M Sodium chloride, 0.1 M BICINE pH 9.0, 20% v/v PEG550 |