7YOR
Recj2 and dCMP complex from Methanocaldococcus jannaschii
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-27 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9791 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 83.600, 175.170, 66.180 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 75.450 - 2.530 |
R-factor | 0.1922 |
Rwork | 0.188 |
R-free | 0.25340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7yik |
RMSD bond length | 0.008 |
RMSD bond angle | 0.924 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.31) |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 175.170 | 2.600 |
High resolution limit [Å] | 2.530 | 2.530 |
Rmerge | 0.094 | 0.662 |
Rmeas | 0.106 | 0.742 |
Rpim | 0.048 | 0.330 |
Total number of observations | 11823 | |
Number of reflections | 61795 | 2392 |
<I/σ(I)> | 12 | 2.6 |
Completeness [%] | 99.8 | |
Redundancy | 4.8 | 4.9 |
CC(1/2) | 0.996 | 0.758 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 12% PEG 400, 50mM HEPES pH 7.6 |