7YOQ
Recj2 and CMP complex from Methanocaldococcus jannaschii
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-27 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9791 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 83.830, 175.630, 66.440 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.907 - 2.265 |
R-factor | 0.2042 |
Rwork | 0.202 |
R-free | 0.25030 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7yik |
RMSD bond length | 0.008 |
RMSD bond angle | 0.908 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.31) |
Phasing software | PHENIX |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 175.630 | 175.630 | 2.320 |
High resolution limit [Å] | 2.260 | 10.130 | 2.260 |
Rmerge | 0.083 | 0.042 | 0.653 |
Rmeas | 0.094 | 0.049 | 0.731 |
Rpim | 0.043 | 0.025 | 0.324 |
Total number of observations | 1870 | 16673 | |
Number of reflections | 87358 | 533 | 3382 |
<I/σ(I)> | 12.1 | 23 | 2.7 |
Completeness [%] | 99.8 | 86.5 | 100 |
Redundancy | 4.8 | 3.5 | 4.9 |
CC(1/2) | 0.996 | 0.994 | 0.799 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 12% PEG 400, 50mM HEPES pH 7.6 |