7YLL
Crystal structure of TTEDbh
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-18 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97929 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 105.196, 105.196, 74.211 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 14.877 - 2.600 |
R-factor | 0.231538208837 |
Rwork | 0.230 |
R-free | 0.26531 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2rdi |
RMSD bond length | 0.008 |
RMSD bond angle | 1.397 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Refinement software | PHENIX (1.12-2829_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 14.880 | 2.770 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 22314 | 2185 |
<I/σ(I)> | 133.9 | |
Completeness [%] | 98.2 | |
Redundancy | 7.1 | |
CC(1/2) | 0.980 | 0.998 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 500 mM NaCl, 5 mM Mg3(PO4)2, 18% [w/v] PEG 3350 |