7YLG
Crystal structure of the chicken Toll-like receptor 15 TIR domain (glutathione adduct)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2022-06-11 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.9793 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 64.625, 64.625, 94.911 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 27.980 - 1.800 |
R-factor | 0.2151 |
Rwork | 0.214 |
R-free | 0.24220 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7ylf |
RMSD bond length | 0.009 |
RMSD bond angle | 0.867 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.830 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 21418 | 1056 |
<I/σ(I)> | 39.8 | 2.3 |
Completeness [%] | 97.8 | 99.5 |
Redundancy | 7.2 | 7.2 |
CC(1/2) | 0.996 | 0.822 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 291 | Dipotassium hydrogen phosphate, sodium dihydrogen phosphate, sodium acetate |