7YKH
Crystal structure of MAGI2 PDZ0-GK domain in complex with phospho-SAPAP1 GBR2 peptide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-08-28 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97917 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.212, 61.540, 65.104 |
Unit cell angles | 90.00, 101.79, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.540 |
High resolution limit [Å] | 2.500 | 6.780 | 2.500 |
Rmerge | 0.107 | 0.056 | 0.629 |
Total number of observations | 108108 | ||
Number of reflections | 14863 | 779 | 723 |
<I/σ(I)> | 8.8 | ||
Completeness [%] | 99.7 | 98.7 | 99.9 |
Redundancy | 7.3 | 6.9 | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 25% w/v PEG 3350, 0.1 M HEPES (pH 7.5) |