7YH3
TRAPPC3 from Thorarchaeota SMTZ1-45
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE TPS 05A |
Synchrotron site | NSRRC |
Beamline | TPS 05A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-04-06 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 68.387, 62.060, 69.324 |
Unit cell angles | 90.00, 100.46, 90.00 |
Refinement procedure
Resolution | 19.480 - 1.700 |
R-factor | 0.2185 |
Rwork | 0.216 |
R-free | 0.25840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7yh2 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.048 | 0.351 |
Rmeas | 0.056 | 0.351 |
Rpim | 0.028 | 0.177 |
Number of reflections | 51122 | 2550 |
<I/σ(I)> | 22.9 | 2.2 |
Completeness [%] | 94.9 | |
Redundancy | 3.8 | |
CC(1/2) | 0.932 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 00 mM HEPES pH 7.5 250 mM Mg(HCO2)2 18% PEG 3350 |