7YH1
Roadblock from Candidatus Prometheoarchaeum syntrophicum strain MK-D1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE TPS 05A |
Synchrotron site | NSRRC |
Beamline | TPS 05A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2021-03-16 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 1 |
Spacegroup name | P 1 |
Unit cell lengths | 48.338, 53.574, 59.856 |
Unit cell angles | 76.65, 75.32, 80.61 |
Refinement procedure
Resolution | 19.940 - 2.690 |
R-factor | 0.2235 |
Rwork | 0.222 |
R-free | 0.26510 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7f8m |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.750 |
High resolution limit [Å] | 2.690 | 2.690 |
Rmerge | 0.049 | 0.185 |
Rmeas | 0.069 | 0.261 |
Rpim | 0.049 | 0.185 |
Number of reflections | 14124 | 1384 |
<I/σ(I)> | 23.7 | 4.4 |
Completeness [%] | 91.6 | |
Redundancy | 1.9 | |
CC(1/2) | 0.952 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 100 mM MES, pH 6.0 250 mM Zn(CH3COO)2 6% PEG 3000 |