7YF1
Structure of FABP at 1.7 Angstroms resolution.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 2009-08-31 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.5 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.305, 54.419, 65.387 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.830 - 1.700 |
R-factor | 0.1698 |
Rwork | 0.169 |
R-free | 0.19670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1g5w |
RMSD bond length | 0.006 |
RMSD bond angle | 0.855 |
Data reduction software | DENZO |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.830 | 1.761 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 15182 | 1456 |
<I/σ(I)> | 27.2 | |
Completeness [%] | 99.8 | |
Redundancy | 1.1 | |
CC(1/2) | 1.000 | 1.000 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 298 | 25% PEG 2000 MME, 0.1 M HEPES pH7.5 |