7YF1

Structure of FABP at 1.7 Angstroms resolution.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU
Temperature [K]	298
Detector technology	CCD
Collection date	2009-08-31
Detector	MAR CCD 165 mm
Wavelength(s)	1.5
Spacegroup name	P 21 21 21
Unit cell lengths	37.305, 54.419, 65.387
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	41.830 - 1.700
R-factor	0.1698
Rwork	0.169
R-free	0.19670
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1g5w
RMSD bond length	0.006
RMSD bond angle	0.855
Data reduction software	DENZO
Data scaling software	SCALA
Phasing software	PHENIX
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	41.830	1.761
High resolution limit [Å]	1.700	1.700
Number of reflections	15182	1456
<I/σ(I)>	27.2
Completeness [%]	99.8
Redundancy	1.1
CC(1/2)	1.000	1.000

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		298	25% PEG 2000 MME, 0.1 M HEPES pH7.5