7YDW
Crystal structure of the MPND-DNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL10U2 |
Synchrotron site | SSRF |
Beamline | BL10U2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-10-16 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 1 |
Unit cell lengths | 37.783, 62.922, 69.085 |
Unit cell angles | 72.58, 89.88, 89.98 |
Refinement procedure
Resolution | 33.440 - 2.470 |
Rwork | 0.245 |
R-free | 0.25360 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7ydt |
RMSD bond length | 0.003 |
RMSD bond angle | 1.181 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | BALBES |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.510 |
High resolution limit [Å] | 2.470 | 2.470 |
Number of reflections | 21839 | 899 |
<I/σ(I)> | 9.5 | 9.5 |
Completeness [%] | 96.0 | |
Redundancy | 3.4 | |
CC(1/2) | 0.968 | 0.894 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | PEG4000, sodium citrate, ammonium acetate |