7YD2
SulE_P44R_S209A
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-04-13 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.979183 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 51.310, 140.260, 58.190 |
| Unit cell angles | 90.00, 101.71, 90.00 |
Refinement procedure
| Resolution | 47.300 - 1.610 |
| Rwork | 0.165 |
| R-free | 0.18120 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 7y0l |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.030 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (v1.16) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 70.130 | 1.650 |
| High resolution limit [Å] | 1.610 | 1.610 |
| Rpim | 0.031 | 0.192 |
| Number of reflections | 102138 | 7066 |
| <I/σ(I)> | 14.6 | |
| Completeness [%] | 98.8 | |
| Redundancy | 6.3 | |
| CC(1/2) | 0.997 | 0.898 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 277 | PEG |
