7Y6Z
RLGSGG-AtPRT6 UBR box (I222)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 193 |
Detector technology | PIXEL |
Collection date | 2019-11-24 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 38.986, 45.754, 86.824 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.670 - 1.598 |
R-factor | 0.238 |
Rwork | 0.234 |
R-free | 0.27140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6lhn |
RMSD bond length | 0.019 |
RMSD bond angle | 1.647 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.670 | 1.655 |
High resolution limit [Å] | 1.598 | 1.598 |
Number of reflections | 10003 | 571 |
<I/σ(I)> | 26.829 | |
Completeness [%] | 93.3 | |
Redundancy | 6.2 | |
CC(1/2) | 0.997 | 0.865 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 0.2 M Calcium acetate hydrate, 20% (w/v) PEG 3350 |