7Y6W

RRGSGG-AtPRT6 UBR box (I222)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	193
Detector technology	PIXEL
Collection date	2019-11-24
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1
Spacegroup name	I 2 2 2
Unit cell lengths	39.170, 45.769, 87.293
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.535 - 1.950
R-factor	0.1961
Rwork	0.192
R-free	0.23030
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6lhn
RMSD bond length	0.010
RMSD bond angle	0.932
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.14_3260: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.020
High resolution limit [Å]	1.890	1.920
Number of reflections	5957	548
<I/σ(I)>	28.64
Completeness [%]	99.0
Redundancy	7.4
CC(1/2)	1.000	0.925

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.5	295	0.2 M Calcium acetate hydrate, 20% (w/v) PEG 3350, pH 7.5