7Y4R
Structure of RclX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100.15 |
Detector technology | PIXEL |
Collection date | 2021-11-26 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.97942 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.170, 92.710, 96.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.610 - 2.510 |
R-factor | 0.2095 |
Rwork | 0.206 |
R-free | 0.26650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5dip |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.19.1_4122) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.540 |
High resolution limit [Å] | 2.500 | 6.780 | 2.500 |
Rmerge | 0.143 | 0.074 | 0.376 |
Rmeas | 0.152 | 0.077 | 0.423 |
Rpim | 0.050 | 0.022 | 0.185 |
Total number of observations | 174870 | ||
Number of reflections | 23999 | 1362 | 972 |
<I/σ(I)> | 6.5 | ||
Completeness [%] | 96.7 | 99.2 | 80.4 |
Redundancy | 7.3 | 11.4 | 3.8 |
CC(1/2) | 0.998 | 0.779 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 287.15 | 0.1 M sodium acetate trihydrate pH 4.6 15.5% (v/v) PEG 300 |