7Y3B
Crystal structure of TRIM7 bound to GN1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17B1 |
Synchrotron site | SSRF |
Beamline | BL17B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2021-10-08 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 0.97934 |
Spacegroup name | P 65 |
Unit cell lengths | 79.768, 79.768, 52.229 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.660 - 1.760 |
R-factor | 0.1655 |
Rwork | 0.163 |
R-free | 0.18890 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6uma |
RMSD bond length | 0.008 |
RMSD bond angle | 1.028 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2-4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.660 | 1.824 |
High resolution limit [Å] | 1.760 | 1.761 |
Rmerge | 0.132 | 1.229 |
Number of reflections | 18832 | 1870 |
<I/σ(I)> | 20.08 | |
Completeness [%] | 99.9 | |
Redundancy | 18.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1 M MES monohydrate pH 6.0, 14% w/v Polyethylene glycol 4,000 |