7Y11
Crystal structure of AtSFH5-Sec14 in complex with egg PA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-03-09 |
Detector | DECTRIS PILATUS3 R 200K-A |
Wavelength(s) | 1.54 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 99.976, 114.252, 112.760 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.050 - 1.950 |
R-factor | 0.2008 |
Rwork | 0.199 |
R-free | 0.23590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1aua |
RMSD bond length | 0.010 |
RMSD bond angle | 1.529 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.020 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.171 | 2.021 |
Rpim | 0.049 | 0.616 |
Number of reflections | 47341 | 4662 |
<I/σ(I)> | 16.2 | 1.45 |
Completeness [%] | 99.8 | 99.9 |
Redundancy | 13.1 | 11.6 |
CC(1/2) | 0.997 | 0.510 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.1 M Bis-Tris propone, pH 6.5, 20% PEG3350 and 0.2 M NaNO3 |