7Y0L
SulE-S209A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-29 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9789 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 51.219, 139.863, 58.101 |
Unit cell angles | 90.00, 101.60, 90.00 |
Refinement procedure
Resolution | 36.070 - 1.290 |
Rwork | 0.154 |
R-free | 0.16720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4q34 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.978 |
Data reduction software | HKL-2000 |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.16) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.310 |
High resolution limit [Å] | 1.290 | 1.290 |
Rpim | 0.241 | |
Number of reflections | 193359 | 9349 |
<I/σ(I)> | 28.5 | |
Completeness [%] | 96.7 | 93.4 |
Redundancy | 6.6 | |
CC(1/2) | 0.993 | 0.925 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | PEG4000 |