7Y01
Crystal structure of ZmMCM10 in complex with 16nt ssDNA at 2.8. Angstrom resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2015-05-05 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 85.180, 85.180, 103.912 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 36.880 - 2.800 |
R-factor | 0.201 |
Rwork | 0.199 |
R-free | 0.24300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ebe |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.126 | 0.702 |
Number of reflections | 11121 | 60687 |
<I/σ(I)> | 14.6 | 2.1 |
Completeness [%] | 99.5 | 98.6 |
Redundancy | 5.4 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION, RECRYSTALLIZATION | 293.15 | 0.2M lithium citrate, 20% PEG 3350 |