7XXU

Macaca fascicularis galectin-10/Charcot-Leyden crystal protein

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-10-31
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97930
Spacegroup name	P 65 2 2
Unit cell lengths	48.530, 48.530, 258.914
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.990 - 1.800
R-factor	0.1876
Rwork	0.184
R-free	0.21720
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5xrg
Refinement software	PHENIX (1.17_3644)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.990	1.840
High resolution limit [Å]	1.800	1.800
Rmerge	0.093	0.379
Number of reflections	17996	1029
<I/σ(I)>	20.1
Completeness [%]	99.9
Redundancy	16.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG