7XWF

RLGSGG-AtPRT6 UBR box (highest resolution)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	193
Detector technology	PIXEL
Collection date	2019-11-24
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1
Spacegroup name	I 2 2 2
Unit cell lengths	39.618, 45.795, 87.085
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	36.060 - 1.451
R-factor	0.1909
Rwork	0.189
R-free	0.20990
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6lhn
RMSD bond length	0.007
RMSD bond angle	0.968
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.14_3260: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	36.060	1.503
High resolution limit [Å]	1.451	1.451
Number of reflections	13083	851
<I/σ(I)>	28.86
Completeness [%]	90.5
Redundancy	7.7
CC(1/2)	0.999	0.921

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		295	0.2 M calcium acetate hydrate, 17 % (w/v) PEG 3350