7XWE
RRGSGG-AtPRT6 UBR box
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 11C |
| Synchrotron site | PAL/PLS |
| Beamline | 11C |
| Temperature [K] | 193 |
| Detector technology | PIXEL |
| Collection date | 2019-12-14 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1 |
| Spacegroup name | P 2 21 21 |
| Unit cell lengths | 46.192, 55.859, 57.323 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 40.010 - 1.598 |
| R-factor | 0.1791 |
| Rwork | 0.177 |
| R-free | 0.20010 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6lhn |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.039 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.010 | 1.655 |
| High resolution limit [Å] | 1.598 | 1.598 |
| Number of reflections | 20140 | 1909 |
| <I/σ(I)> | 12.92 | |
| Completeness [%] | 99.4 | |
| Redundancy | 5.9 | |
| CC(1/2) | 0.988 | 0.720 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 295 | 0.2 M MgCl2 hexahydrate, 0.1 M sodium HEPES pH7.5, and 30% (v/v) PEG 400 |
