7XRZ
Crystal structure of BRIL and SRP2070_Fab complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.00004 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 93.828, 75.239, 152.231 |
Unit cell angles | 90.00, 99.67, 90.00 |
Refinement procedure
Resolution | 42.740 - 2.100 |
R-factor | 0.2164 |
Rwork | 0.214 |
R-free | 0.26840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1m6t 1f58 |
RMSD bond length | 0.004 |
RMSD bond angle | 1.319 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.21) |
Phasing software | PHASER (2.6.1) |
Refinement software | REFMAC (5.8.0232) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.640 | 48.640 | 2.160 |
High resolution limit [Å] | 2.100 | 9.150 | 2.100 |
Rmerge | 0.063 | 0.019 | 0.645 |
Rmeas | 0.080 | 0.024 | 0.815 |
Rpim | 0.049 | 0.015 | 0.490 |
Total number of observations | 134803 | 1787 | 10143 |
Number of reflections | 57858 | 705 | 4489 |
<I/σ(I)> | 10.8 | 44.2 | 1.5 |
Completeness [%] | 94.9 | 90 | 94.7 |
Redundancy | 2.3 | 2.5 | 2.3 |
CC(1/2) | 0.996 | 0.997 | 0.568 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 277.15 | PEG 6000, Tris-HCl |