7XRX
insulin-cleaving membrane protease-ICMP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NFPSS BEAMLINE BL18U |
Synchrotron site | NFPSS |
Beamline | BL18U |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2017-12-15 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.987 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 87.927, 78.141, 99.916 |
Unit cell angles | 90.00, 113.52, 90.00 |
Refinement procedure
Resolution | 34.372 - 1.882 |
R-factor | 0.1479 |
Rwork | 0.146 |
R-free | 0.18650 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 0.837 |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.372 | 1.970 |
High resolution limit [Å] | 1.882 | 1.900 |
Number of reflections | 97961 | 54651 |
<I/σ(I)> | 14.3 | |
Completeness [%] | 99.4 | |
Redundancy | 5.8 | |
CC(1/2) | 0.839 | 0.839 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291.15 | 1.6 M sodium citrate tri-basic dihydrate at pH 6.5 |