7XRE
Crystal structure of DgpA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2021-10-03 |
Detector | DECTRIS EIGER R 4M |
Wavelength(s) | 0.9875 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 94.790, 130.760, 206.680 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 17.076 - 2.760 |
R-factor | 0.2377 |
Rwork | 0.235 |
R-free | 0.29420 |
Structure solution method | SAD |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | AutoSol |
Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.700 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.182 | |
Number of reflections | 65488 | 1013 |
<I/σ(I)> | 10.6 | |
Completeness [%] | 98.2 | |
Redundancy | 11.5 | |
CC(1/2) | 0.750 | 0.800 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.2 M magnesium formate and 20% PEG 3350 |