7XPW
Structure of OhTRP14
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-01-06 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.97930 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 34.772, 44.912, 38.491 |
Unit cell angles | 90.00, 115.10, 90.00 |
Refinement procedure
Resolution | 34.860 - 1.770 |
R-factor | 0.1718 |
Rwork | 0.168 |
R-free | 0.23160 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1wou |
RMSD bond length | 0.016 |
RMSD bond angle | 1.602 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.800 |
High resolution limit [Å] | 1.770 | 1.770 |
Rmerge | 0.052 | 0.181 |
Number of reflections | 10429 | 10429 |
<I/σ(I)> | 28.535 | |
Completeness [%] | 98.4 | |
Redundancy | 6.3 | 6.1 |
CC(1/2) | 0.966 | 0.966 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.9 | 289 | 30% PEG 3350, 0.1M Bis-tris PH 5.9 |