7XPT
Crystal structrue of MtdL:GDP:Mn soaked with GDP-Glc
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-06-18 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 162.275, 98.825, 58.102 |
Unit cell angles | 90.00, 96.77, 90.00 |
Refinement procedure
Resolution | 57.700 - 2.000 |
R-factor | 0.2174 |
Rwork | 0.215 |
R-free | 0.25900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7xpr |
Data reduction software | XDS |
Data scaling software | Aimless (0.7.7) |
Phasing software | PHASER |
Refinement software | PHENIX (1.19_4092) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 80.570 | 80.570 | 2.050 |
High resolution limit [Å] | 2.000 | 8.940 | 2.000 |
Rmerge | 0.097 | 0.039 | 0.919 |
Rmeas | 0.106 | 0.043 | 1.000 |
Rpim | 0.041 | 0.017 | 0.388 |
Total number of observations | 352445 | 4039 | 26413 |
Number of reflections | 55455 | 708 | 4201 |
<I/σ(I)> | 11.1 | 30.6 | 1.7 |
Completeness [%] | 90.2 | 97.9 | 93.7 |
Redundancy | 6.4 | 5.7 | 6.3 |
CC(1/2) | 0.998 | 0.998 | 0.879 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 283 | 0.1 M tri-sodium citrate pH 5.6, 10% (w/v) PEG 4000, 10% (w/v) isopropanol |